VMK OPTOELEKTRONIKA

A device for preparing metal samples for spectral analysis. For the preparation of metal samples, an emery cloth or paper with a given size and abrasive material is used. The rotation speed is 1500 revolutions per minute. A quick stop of the motor is provided by an automatic control unit. There is a version in a housing made of composite materials with two discs, each can have its own type of abrasive.

A remote-controlled atomizer of powder samples with automatic change of revolver-type samples with arc excitation of the spectrum. It consists of an automatic tripod "Carousel" for arc spectral analysis and a spectroanalytic generator "Ball Lightning"– 40A fully compatible with the expert software system "ATOM" and the MAES analyzer.

The generator is designed to produce an electric arc and spark discharge in atomic emission spectral analysis installations. The generator is designed specifically for use in spectral analysis of samples of complex composition for simultaneous determination of impurity and alloying components in a wide range of concentrations.

During operation, the steam generator of metal samples "Aspect" provides control of all devices of the atomic emission spectral analysis complex - the MAES analyzer, the Ball Lightning generator, the inclusion of external devices; A spark unipolar discharge is excited between a tungsten counterelectrode and the surface of the test samples - ingots of precious metals or other metal samples; The intensity of erosion of the sample surface is regulated by changing the repetition frequency and power of spark pulses generated by a computer-controlled semiconductor spark generator; The stability and quality of the frisking is monitored using a built-in spectrometer via optical fiber; An adjustable flow of high-purity argon passes through the spark discharge zone in a sealed discharge chamber, picks up sample particles obtained by spark erosion of the surface and transfers them in the form of an aerosol to the area of the mixer/sprayer of the inductively coupled plasma torch of the optical emission spectrometer.; The flow of high-purity argon is supplied, controlled and regulated by a microprocessor-controlled mass flow controller in the range from 0.5 to 3 l/min. Feed stability 0.01 l/min.

The laser source is designed to excite atomic emission spectra when performing qualitative spectral analysis of hard rocks - metals, minerals, glasses and others. The source is based on a two-pulse YAG: Nd laser with electro-optic Q-switching operating at the main wavelength of 1064 nm. The duration of each pulse is no more than 10 ns, and the delay between them is adjustable from 0 to 60 microseconds. The possibility of the laser beam to focus on an area of 300 to 1000 microns makes it possible to conduct microanalysis of inclusions, perform two-dimensional scanning of the surface or locally analyze samples with virtually no damage to the surface. A significant advantage of the laser source is the expressiveness and lack of special sample preparation for a wide range of conductive and non-conductive materials. Visual observation and pointing of the beam at the sample is carried out using a stereoscopic microscope integrated into the system, as well as a high-resolution digital video camera with image transmission to a computer. Moving the instrument table with a fixed sample is possible both manually for adjustment, and with the help of stepper motors in two coordinates during analysis, which provides surface scanning and spectrum recording with reference to the video image. The installation can be used in conjunction with any spectral devices – "Grand", "Aspect", "Express", "Hummingbird-2", STE-1, DFS-458, MFS-8, PGS-2 and others. The laser source is designed to excite atomic emission spectra when performing high-quality spectral analysis of hard rocks – metals, minerals, glasses and others.

The flame spectrometer is designed for rapid determination of a wide range of concentrations (up to 8 orders of magnitude) of sodium, lithium, potassium, calcium, barium, caesium, rubidium in technological solutions. The excitation of atoms occurs in an air-acetylene flame. The device consists of a three-slit burner with flame control, a pneumatic sprayer, a spray chamber, an optical radiation input system into the "Hummingbird-2" spectrometer and an automatic air and acetylene supply system, with the possibility to control and adjust gas flow. The use of a three-slit burner provides increased flame temperature over the central slit of the burner due to the external flame layers. This makes it possible to determine low concentrations of calcium and barium. At the same time, it remains the possibility to determine impurities in highly concentrated solutions without clogging the burner slots. The lighting system of the spectrometer is mirror-lens, thanks to this, radiation collected from both sides of the burner is introduced into the polychromator.

Diesel engine oil spectrometric analysis system "EXPRESS-OIL" is designed to analyze engine oils according to GOST 20759 and determine the concentration of wear elements of rubbing diesel parts, contaminants and additives in diesel engine oils during scheduled maintenance and repair of traction rolling stock in locomotive repair depots, as well as electronic accounting and analysis of dynamics data the content of wear elements in engine oils for each locomotive, as well as the determination of the composition of metals and alloys according to GOST, greases (according to CTCH-28/4, CTCHS-53) and other materials.

The MAES analyzer is a modern means of measuring the intensities of spectral lines and then calculating the concentrations of the elements to be determined.

The plasmatron is designed for direct atomic emission spectral analysis of powder samples. The excitation of atoms occurs in a DC argon arc plasma. Weak matrix effects and low detection limits make it possible to use this excitation source for the analysis of various samples, both with mineral and organic matrix.

The video camera and servos of the electrode holders built into the tripod are designed to automatically maintain the interelectrode gap during the evaporation of the sample by computer analysis in real time of the image of the arc discharge, as well as the initial setting of this gap relative to the optical axis. The electrode holders are cooled with water using a closed-cycle cooling unit.