Specialized X-ray wavelength dispersive analyzer ARF-7

The CR-1B reactor is an automated chemical reactor with thermostat, stirrer and reagent management system. To control the reactor, specialized software is used (supplied with the reactor). This reactor may be of most interest for laboratory research for routine synthesis of nano/microparticles (e.g. vaterite), as well as experimental scaling tests with a view to further transferring it to production facilities.

The spectrometer was created according to the Cherni-Turner scheme based on a flat diffraction grating and an MAES analyzer with one line of photodetectors. It has increased photometric accuracy due to cooling and temperature stabilization of the photodetector range, as well as due to its shell-less design, in which there is no re-reflection of radiation on the cover glass and the background level in the recorded spectrum decreases. The optical scheme and design of the spectrometer are optimized to obtain a high-quality spectrum with a low level of background radiation in any of the regions lying in the spectral range of 190-1100 nm. The choice of the working area is carried out by changing and rotating the diffraction gratings. The sealed case of the spectrometer is filled with an inert gas. The radiation is injected into the spectrometer using a quartz capacitor or a fiber-optic cable with an SMA-905 connector. The optical scheme and design of the spectrometer are protected by patents.

The X-ray fluorescence spectrometer SPECTROSCAN MAX-GF1(2)E-C combines two methods of detecting an analytical signal: diffraction on a crystal (wave dispersion - WDX) and energy dispersion (EDX) method, as well as sample delivery adapted for the analysis of large-size images. The collimation of the primary radiation of the X-ray tube and the special design of the sample presentation make it possible to analyze the sample over an area of 1 cm2 in 1 mm increments, and thus investigate the distribution of elements over an area. The spectrometer is designed to determine the contents of elements in the range from Ca to U in substances in solid, powdery, dissolved states, as well as deposited on the surface or deposited on filters. With the help of fixed energy dispersion channels, any one or two additional elements in the range from magnesium (Mg) to calcium (Ca) can be determined. With the help of this modification of the spectrometer, forensic and customs examinations, judicial and forensic medical examinations, as well as art-historical examinations are carried out.

The spectrometer is designed to determine the contents of elements in the range from Na to U in substances in solid, powdery, dissolved states, as well as deposited on the surface or deposited on filters. The principle of operation of the X-ray spectrometer is based on irradiation of the sample with primary radiation from an X-ray tube, measurement of the intensity of secondary fluorescent radiation from the sample at wavelengths corresponding to the elements to be determined, and subsequent calculation of the mass fraction of these elements according to a pre-constructed calibration characteristic, which is the dependence of the content of the element to be determined on the measured intensity. Secondary fluorescent radiation is decomposed into a spectrum using a crystal analyzer. Due to this, the X-ray fluorescence spectrometer has a high resolution, and therefore the ability to accurately analyze complex multicomponent substances.

Designation SNOL 11.47.4/2.5 P I2 Temperature, oS 250 Camera power, kW 16 Mandrel length 1200...4600 Opening the lid electric drive

The dual-view plasma spectrometer can record any spectral line simultaneously at high resolution in the concentration range from fractions of ppb up to tens of percent and offers a wide range of options for any research task. Designed for the analysis of almost any type of environmental samples – water, soil, precipitation. Quick switching to work. It does not require a long warm-up. Low argon consumption. Easy to use.

During operation, the steam generator of metal samples "Aspect" provides control of all devices of the atomic emission spectral analysis complex - the MAES analyzer, the Ball Lightning generator, the inclusion of external devices; A spark unipolar discharge is excited between a tungsten counterelectrode and the surface of the test samples - ingots of precious metals or other metal samples; The intensity of erosion of the sample surface is regulated by changing the repetition frequency and power of spark pulses generated by a computer-controlled semiconductor spark generator; The stability and quality of the frisking is monitored using a built-in spectrometer via optical fiber; An adjustable flow of high-purity argon passes through the spark discharge zone in a sealed discharge chamber, picks up sample particles obtained by spark erosion of the surface and transfers them in the form of an aerosol to the area of the mixer/sprayer of the inductively coupled plasma torch of the optical emission spectrometer.; The flow of high-purity argon is supplied, controlled and regulated by a microprocessor-controlled mass flow controller in the range from 0.5 to 3 l/min. Feed stability 0.01 l/min.

NanoEducator II, despite its compactness and ease of operation, supports all basic techniques of atomic force and scanning tunneling microscopy, so it can be used for any routine AFM and STM measurements and experiments in scientific research. Here are the results of some experiments in various scientific applications: Study of atomic structures Study of metallic nanostructures Study of magnetic structures Study of polymer objects Study of biological objects Study of carbon nanomaterials

Vacuum spectrometers are designed for rapid analysis of alloys based on iron, copper, aluminum and other metals in factory and research laboratories, including the determination of elements having analytical lines in the field of vacuum ultraviolet (VUV) (for example, S, P and C in steels).

The MS-1104E spectrometer is characterized by high performance and accuracy of Mössbauer measurements achieved through the use of “compressed” geometry, as well as the use of highly efficient and selective resonant scintillation detection units that improve the energy resolution of resonance absorption lines by up to 30%. The technique of software and hardware stabilization of the spectrometric path developed and used in the spectrometer allows for long-term Mossbauer measurements without manual adjustment. The method of modulation in the specified speed intervals can significantly increase the sensitivity and expressiveness of measurements and reduce the time to determine the magnitude of the effects of resonant absorption by tens of times in the study of temperature phase transitions with a low concentration of resonant elements. The electronic components of the spectrometer are developed on the basis of a modern element base using programmable logic matrices and microprocessors. Adjustable spectrometric paths and high-voltage power supplies of the PMU are integrated into detection units, modulator driver modules and multi-channel storage are made in the ISA standard and are located in the processor unit of the computer. Setting and monitoring of all parameters of the spectrometer and processing of the measured spectra is carried out from the operating windows of the control and processing programs. Since 2000, more than ten spectrometers of this type have been supplied to leading scientific organizations in Russia and neighboring countries. One of the few industrial applications of Mössbauer spectroscopy should be noted - the development and supply to the Volgodonsk NPP of certified MS-1104Em methods and spectrometer for monitoring corrosion processes in the heat exchange circuits of the VVER-1000 reactor.

Vacuum spectrometers are designed for rapid analysis of alloys based on iron, copper, aluminum and other metals in factory and research laboratories, including the determination of elements having analytical lines in the field of vacuum ultraviolet (VUV) (for example, S, P and C in steels).

The ultimate display quality is ensured by the use of built-in acoustic and vibration isolation, thermal stabilization, the industry's best sensitivity of the optical recording system and the unique design of the scanning probe system, which allows achieving atomic resolution in routine measurements. In the basic configuration, 50+ AFM techniques are available, including the HybriD method, which allows conducting all cutting-edge nanomechanical, electrical and magnetic studies. Intelligent ScanTronic™ algorithm for one-click optimization of scanning parameters, which allows for perfect relief measurements using the amplitude-modulation method, regardless of the operator's experience. Automated examination of multiple samples using a simple user interface to create a point-by-point scanning scenario and a database for stored received images. Control of samples with dimensions up to 200×200 mm and thickness up to 40 mm at any point of the surface with a positioning accuracy of 1 micron. Wide customization possibilities: installation of additional optical equipment, development of specialized sample holders, combination with a transport system, automation of measurements and data analysis in accordance with customer requirements.

Atomic Emission Complex "Grand Globula" includes a spectrometer "Grand", a spectroanalytic generator "Ball Lightning" and a tripod "Globula". It allows the analysis of various substances and materials in arc and spark discharges in air, for example according to GOST 17818.15-90 "Graphite. Spectral analysis method", GOST 9717.1-82 "Copper. A method of spectral analysis based on metallic standard samples with photoelectric spectrum registration" and other MVIS.