Accessories

Silicone hose with thermal insulation and an internal diameter of 8 mm is used to connect the A160 and A300 circulation coolers with the W series thermostats or to external consumers.

The laser source is designed to excite atomic emission spectra when performing qualitative spectral analysis of hard rocks - metals, minerals, glasses and others. The source is based on a two-pulse YAG: Nd laser with electro-optic Q-switching operating at the main wavelength of 1064 nm. The duration of each pulse is no more than 10 ns, and the delay between them is adjustable from 0 to 60 microseconds. The possibility of the laser beam to focus on an area of 300 to 1000 microns makes it possible to conduct microanalysis of inclusions, perform two-dimensional scanning of the surface or locally analyze samples with virtually no damage to the surface. A significant advantage of the laser source is the expressiveness and lack of special sample preparation for a wide range of conductive and non-conductive materials. Visual observation and pointing of the beam at the sample is carried out using a stereoscopic microscope integrated into the system, as well as a high-resolution digital video camera with image transmission to a computer. Moving the instrument table with a fixed sample is possible both manually for adjustment, and with the help of stepper motors in two coordinates during analysis, which provides surface scanning and spectrum recording with reference to the video image. The installation can be used in conjunction with any spectral devices – "Grand", "Aspect", "Express", "Hummingbird-2", STE-1, DFS-458, MFS-8, PGS-2 and others. The laser source is designed to excite atomic emission spectra when performing high-quality spectral analysis of hard rocks – metals, minerals, glasses and others.

It is intended for sample preparation when examining samples using an IR microscope and mirror reflection prefixes. Allows you to shape a thin layer (up to several microns) to various objects: polymer fragments, microparticles of LCP, powdery substances, fibers, etc. The resulting thin layers on mirror plates made of alloy steel are investigated by the double transmission method – when the radiation that has passed through the layer of matter is reflected from the surface of the plate and passes through the substance again. The spectra recorded by this method are completely identical to the transmission spectra obtained, for example, after pressing substances with KBr. The advantages in this case are: - speed of sample preparation - there is no need to use hydraulic and manual presses and molds, grinding mortars, etc. - no need to use high-purity KBr or petroleum jelly oil - the sample is not lost and, if necessary, can be examined by other methods - when using an IR microscope, it is possible to “scan” the resulting thin layer to select the most informative area, and also, if the layer is heterogeneous in composition, to obtain the spectral characteristics of its components.

Vibration velocity sensors with a current output DVST-1 are designed to convert the RMS value of the vibration velocity of an object into a standard current signal of 4-20 mA.

The main advantage of the PRIZ prefix is the possibility of obtaining well–defined spectra of micro-objects after giving them the shape of a thin layer on mirror-polished metal plates (in the mode of the so-called double passage, when radiation twice penetrates through the layer of matter, reflecting from the mirror-substrate). The presence of a visual control system with a built-in video camera significantly increases the information content when setting up and the reliability of the results obtained. With the help of the prefix, it is also possible to register the reflection spectra of bulk samples and solid objects of arbitrary geometry in native form, including pharmaceuticals in the form of tablets, powders and granules, polymer fragments, LCP, films deposited on the surface. Technical specifications Transmission in the operating range of the spectrum, % of the input signal at least 40 The recommended number of scans when registering spectra is 25 Spectrum registration time at 25 scans (resolution 4 cm-1), sec 30 Minimum initial dimensions of a solid sample, mm 0.2 × 0.2 The maximum area of the solid sample, mm 20X20X10 Variable focus range, mm 10 The diameter of the focus spot, mm 3 The angle of incidence of radiation (central beam) on the sample in the ZDO 45o mode Micro lens magnification / total magnification of the 4X visual channel Field of view of the optical system, mm 2 X 2.5 The resolution of the digital video camera is 640x480 Overall dimensions, mm 140×105×160 Weight, kg 1.16

It is designed for measurement by the method of disturbed total internal reflection with simultaneous visualization of a micro-object on an integrated and external monitor, as well as by the method of mirror-diffuse reflection with an angle of incidence of 45o at the upper location of the sample. The prefix in the mode of a single NIP is used to register absorption spectra: liquids of any degree of viscosity (solutions, suspensions, oils, etc.), including those with high chemical activity; solid objects of arbitrary shape, including samples with very high hardness (any polymers, fragments of paint coatings, etc.); powdery substances, including powders with very high hardness (drugs, pharmaceuticals, explosives, inorganic compounds); samples in the form of thin tapes; samples in the form of fibers. The maximum hardness and chemical resistance of the diamond significantly expand the possibilities of the method; there is no need for periodic replacement of the crystal. The set-top box allows you to register spectra without time–consuming sample preparation, and the presence of a visual inspection system of the studied surface with a high-quality video camera and a built-in high-definition mini-monitor increases efficiency when working with small samples - fragments of thin fibers, microparticles, etc. The built-in monitor has the functions of digital 10X zoom, inverting, etc. The image can be simultaneously displayed on the computer screen (using a USB interface) and then saved as a file. The removable flange provides a quick and convenient sample change and cleaning of the crystal surface. The design with a diamond element protruding above the base plane of the NPVO allows you to study samples with sufficiently large overall dimensions. The high quality and repeatability of the results is achieved due to the absence of the influence of the thickness of the substance layer on the shape of the spectrum and the intensity of the absorption bands. The sample retains its original physicochemical properties and, if necessary, can be further investigated by other methods. The universal attachment clamp is equipped with a precision lever mechanism for quickly lowering the tip and a micrometer screw that allows you to pre–set the optimal degree of pressure - this ensures quick sample change and repeatability of the results during measurements. For convenience when working with liquid and paste-like samples, as well as in the ZDO mode, it is possible to rotate the clamping console by 180o. The console is equipped with two replaceable tips – with a spherical working part and with a flat hinged head. The high hardness of the diamond allows the use of large clamping forces, which is the determining factor for obtaining high-quality spectra. A replacement table is used to register the specular and diffuse reflection spectra. The sample is located on the subject plane of the investigated surface downwards. The method is used to determine the spectral characteristics of optical parts, thin tapes on the surface, crystals, and other large solid objects of arbitrary shape and size.

Basic properties Wide frequency range; Small VSWR values. Operating conditions Operating temperature range from minus 10 to 50 ° C; The relative humidity of the air is up to 98% at a temperature of 25 ° C. Technical specifications Waveguide cross section, mm 5.2×2.6 Type of coaxial connector (according to GOST RV 51914-2002) IP Frequency range, GHz 37.50-50.00 VSWR 1.45

Silicone hose with thermal insulation and an internal diameter of 10 mm is used to connect circulating coolers and thermostats of the CRYO-W series to external consumers or is used as a jumper hose

The main difference between this set-top box and the universal set-top box of the NPVO and ZDO is that a prism is used as a working element of the MNPVO, which allows to obtain several reflections from the area of contact with the sample under study, which leads to an improvement in the quality of the spectrum and an increase in the sensitivity of the method (absorption bands become more pronounced). The registration of specular and diffuse reflection spectra (ZDO) is not provided on this set-top box. The MNPVO prefix is effective in registering the absorption spectra of samples whose dimensions (number) are sufficient to ensure contact with the entire area of the working face of the prism: * liquids of any degree of viscosity (solutions, suspensions, oils, etc.); * solid elastic samples (polymer fragments of sufficiently large size, rubbers, plastics, etc.); * powdered samples in quantities sufficient to be applied to the entire surface and samples in the form of thin tapes; The universal clamp is equipped with a precision lever mechanism for quickly lowering the tip and a micrometer screw that allows you to pre–set the optimal degree of pressure - this ensures quick sample change and repeatability of the results during measurements. For convenience when working with liquid and paste-like samples, it is possible to rotate the clamping console by 180o. Note: the MNPVO prefix does not exclude the possibility of registering the spectra of samples whose dimensions are smaller than the area of the working face of the prism (the presence of a visual inspection system of the surface under study increases convenience when working with small-sized objects), but the overall effectiveness of the method is significantly lower than when using the universal NPVO and ZDO prefix. Transmission in the operating range of the spectrum, % of the input signal of at least 25 · The recommended number of scans when registering spectra is 25 · Spectrum registration time at 25 scans (resolution 4 cm-1), 30 seconds · The depth of penetration of radiation into the sample, microns 5 – 15 · Minimum area of a solid sample, mm2 1 · Minimum volume of the test liquid, ml 0.3 · The permissible pH range of the analyzed objects is from 5 to 9 · Crystal substrate material ZnSe CVD, Ge · Diameter of the focus spot, mm 3 · Number of reflections 3 · The size of the working face of the prism, mm 21 X 6 · Magnification of the 4X micro lens · Total magnification of the visual channel 75X · Field of view of the optical system, mm 2 X 2.5 · Digital video camera resolution 640 X 480 · Overall dimensions, mm 145×125×240 · Weight, kg 2

The set of devices is designed to install five working viscometers in a vertical position in the bath of the VIS T 06 liquid thermostat when they are verified.