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A set-top box with a cooled MST detector
A set-top box with a cooled MST detector
To achieve the maximum sensitivity during measurements, a special prefix is used to the FT-801 Fourier spectrometer, which is an optical unit with a built-in highly sensitive MST detector cooled with liquid nitrogen. The set-top box is installed in the cuvette compartment of the spectrometer and connected to the corresponding external electrical port, the detector is turned on programmatically. In this case, the sensitivity of the method increases many times (up to 20) – depending on the type of standard uncooled detector in the spectrometer). The speed of recording spectra is also increasing. The operating time after filling the cryostat (200 ml capacity) with liquid nitrogen is at least 6 hours. Increasing the sensitivity of the spectrometer using a prefix with an MST detector may be required for many applications: in fiber spectroscopy, when recording emission spectra of low-power emitters, in trace gas analysis with high spectral resolution, when determining the presence of impurities in samples in ultra-low concentrations, when using multi-pass gas cuvettes, etc. In the picture: on the left in the cuvette compartment there is a capler with fiber from Art photonics GmbH, Berlin, Germany, on the right there is a prefix with an MST detector. Technical specifications The recommended number of scans when registering spectra is 16 Spectrum registration time at 50 scans (resolution 4 cm-1), sec 20 Cryostat capacity, 200 ml Working time after filling the cryostat, 6 hours Overall dimensions, mm 225×175×75 Weight, kg 1.45
SIMEKS
Novosibirsk
Produced in: Novosibirsk
NTEGRA NANO IR
NTEGRA NANO IR
NT-MDT Spectrum Instruments is an INTEGRA Nano IR–scattering scanning near‑field optical microscope (s-NSOM) designed for the infrared spectral range. The AFM probe is located in the focus of an optical system that directs the IR laser radiation to the sample and collects the optical response. The collected radiation is sent to the Michelson interferometer for optical analysis. The far-field component of the collected signal is suppressed by synchronous detection. The INTEGRA Nano IR system allows detecting the amplitude and phase of the near-field signal. The spatial resolution of the resulting reflection and absorption contrasts is approximately 10 nm and is determined only by the size of the tip of the probe.
Produced in: Moscow, Zelenograd
Liquid flask with adjustable thickness of the test liquid layer
Liquid flask with adjustable thickness of the test liquid layer
A liquid flask with an adjustable layer thickness of the liquid under study is made in the form of an optical-mechanical attachment installed in the cuvette compartment of the FT-801 spectrometer. It contains focusing optics, removable holders of two windows-substrates with a diameter of 10 mm and two adjusting screws placed on the upper panel of the console housing and designed to set the required gap between the windows. A liquid of any degree of viscosity is pre-applied in the form of a small drop to the lower window and then, in the process of smooth convergence of the windows, evenly fills the gap between them. By rotating the adjusting screws and observing the transmission spectrum online, the user has the opportunity to set the desired thickness of the liquid layer, guided by the overall intensity of the entire spectrum or by the intensity of specific absorption bands. In the presence of calibration, which is easy to create using the ZaIR 3.5 program for several samples with a known concentration, the cuvette allows quantitative measurements. The flask is indispensable in the analysis of mixtures containing impurities in small proportions. Technical specifications Transmission in the operating range of the spectrum, % of the input signal at least 50 The recommended number of scans when registering spectra is 16 Time of spectrum registration at 16 scans (resolution 4 cm-1), sec 20 Minimum volume of the studied liquid, mm3 1 The diameter of the focus spot, mm 3 Overall dimensions, mm 200×90×160 Weight, kg 1,1 The figure shows several spectra of the viscous lubricant "Buxol", illustrating the process of selecting the thickness of the sample layer between the windows. The measurement process has a high expressiveness and reproducibility, inexpensive replaceable substrate windows are used, the system is easy to configure and clean, a very small amount of sample is required to obtain high-quality spectra.
SIMEKS
Novosibirsk
Produced in: Novosibirsk
Infrared Laser 780 nm KLM-780-150
Infrared Laser 780 nm KLM-780-150
CDL lasers of the KLM-780-150 series are optimal sources of continuous radiation for the construction of control and automation systems, for scientific and medical purposes.
FTI-Optronik
Saint Petersburg
Produced in: Saint Petersburg
PRIZ - a reflection prefix with the lower position of the sample and visualization of the object under study on the monitor
PRIZ - a reflection prefix with the lower position of the sample and visualization of the object under study on the monitor
The main advantage of the PRIZ prefix is the possibility of obtaining well–defined spectra of micro-objects after giving them the shape of a thin layer on mirror-polished metal plates (in the mode of the so-called double passage, when radiation twice penetrates through the layer of matter, reflecting from the mirror-substrate). The presence of a visual control system with a built-in video camera significantly increases the information content when setting up and the reliability of the results obtained. With the help of the prefix, it is also possible to register the reflection spectra of bulk samples and solid objects of arbitrary geometry in native form, including pharmaceuticals in the form of tablets, powders and granules, polymer fragments, LCP, films deposited on the surface. Technical specifications Transmission in the operating range of the spectrum, % of the input signal at least 40 The recommended number of scans when registering spectra is 25 Spectrum registration time at 25 scans (resolution 4 cm-1), sec 30 Minimum initial dimensions of a solid sample, mm 0.2 × 0.2 The maximum area of the solid sample, mm 20X20X10 Variable focus range, mm 10 The diameter of the focus spot, mm 3 The angle of incidence of radiation (central beam) on the sample in the ZDO 45o mode Micro lens magnification / total magnification of the 4X visual channel Field of view of the optical system, mm 2 X 2.5 The resolution of the digital video camera is 640x480 Overall dimensions, mm 140×105×160 Weight, kg 1.16
SIMEKS
Novosibirsk
Produced in: Novosibirsk
Reflection prefix PO-45 V
Reflection prefix PO-45 V
It is intended for express analysis of various types of solid opaque samples, including polymer films and fragments, paint coatings, finished dosage forms in the form of tablets, optical parts and semiconductor materials. • The sample is located on the subject plane of the investigated surface downwards, the angle of incidence of the central beam on the sample is 45 ° • The diameter of the focus spot is 3 mm • Allows you to explore objects of any shape and size • When using a mini-press, it allows you to examine samples in the form of a thin layer rolled out on a mirror plate made of alloy steel (radiation passes through the substance layer twice, reflecting from the mirror surface) • Not used: for the study of bulk and liquid substances
SIMEKS
Novosibirsk
Produced in: Novosibirsk
IR Laser Module KLM-B808-x-5 808nm
IR Laser Module KLM-B808-x-5 808nm
Laser modules of the KLM-B808-x-5 series are optimal sources of coherent radiation for the construction of control and automation systems, alignment and marking devices, for scientific and medical purposes.
FTI-Optronik
Saint Petersburg
Produced in: Saint Petersburg
Infrared Laser 808 nm KLM-808-x
Infrared Laser 808 nm KLM-808-x
CDL lasers of the KLM-808-x series are optimal sources of continuous radiation for the construction of control and automation systems, for scientific and medical purposes.
FTI-Optronik
Saint Petersburg
Produced in: Saint Petersburg
Mold for the manufacture of tablets with KBr diameter of 13 mm
Mold for the manufacture of tablets with KBr diameter of 13 mm
It is intended for the preparation of samples in the form of compressed tablets consisting of the test substance in a mixture with microcrystalline potassium bromide (KBr). The mold is used in combination with the hydraulic press GP 200-13. - the mold is made of high-quality alloy hardened steel - to obtain better compressed tablets with KBr, the mold can be pumped out using a pre-vacuum pump. The customer can purchase the pump independently, or order it from the NPF “SIMEX”. Pumping out the mold is not necessary for most studies. - the kit includes a special dispenser for placing the optimal amount of the pressed mixture in the mold - to install the finished samples in the spectrometer, a holder of KBr tablets and D13mm substrate windows is used
SIMEKS
Novosibirsk
Produced in: Novosibirsk
Reflection prefix PO-15 V
Reflection prefix PO-15 V
Designed for the study of various types of solid samples, including optical and semiconductor materials, precious stones and other objects of arbitrary shape • The sample is located on the subject plane of the investigated surface downwards, the angle of incidence of the central beam on the sample is 15 ° • Allows you to examine samples of small sizes (the diameter of the test area is from 1 mm) • The set-top box is equipped with a set of replaceable diaphragm holders for samples of different sizes • When using a mini-press, it allows you to examine samples in the form of a thin layer rolled out on a mirror plate made of alloy steel (radiation passes through the substance layer twice, reflecting from the mirror surface) • Not used: for the study of bulk and liquid substances
SIMEKS
Novosibirsk
Produced in: Novosibirsk
Optical system for recording spectra of substances located in remote closed volumes
Optical system for recording spectra of substances located in remote closed volumes
Designed for monitoring processes in reactors, vacuum chambers, gas pipelines, etc.
SIMEKS
Novosibirsk
Produced in: Novosibirsk
Optical set-top box for working with light-guide IR probes
Optical set-top box for working with light-guide IR probes
FT-801 IR Fourier spectrometers can additionally be equipped with a special optical set-top box that allows efficient use of light-guide systems. 4 types of light-guide probes allow measuring transmission and reflection spectra in solid, liquid and gaseous media Modern IR light guides have high intrinsic transmittance and sufficient mechanical strength, which makes it possible to transfer measurements from the laboratory directly to production - to control the flow of technological processes, check the quality of raw materials and finished products. Application areas: · Chemical and microbiological industry · Pharmaceutical industry · Medicine and Cosmetology · Food industry · Petroleum products, fuels and lubricants · Criminology
SIMEKS
Novosibirsk
Produced in: Novosibirsk