NPF "META-KHROM"

When analyzing gases dissolved in transformer oil using the ARP method (equilibrium vapor analysis), it is necessary to first fill a syringe with transformer oil with a carrier gas, and then, after achieving an equilibrium distribution of gases dissolved in oil between the liquid and gas phases, introduce the gas phase into the chromatograph (blow out the doses of the chromatograph dispenser tap). Moreover, the operations of filling the syringe and entering the sample are performed without air access. When filling the syringe, it is possible to fix the syringe stem at a certain volume. technical specifications The volume of syringes is 20 or 50 ml. The pressure at the outlet of the syringe filling line with argon is 0.5 atm. The range of ratios of volumes of the gas phase and oil (Vg/Vm) is from 0 to 1.5.

The gas chromatograph "Kristallux-4000M" is fully automated, starting from sample input and ending with chromatographic information processing, including the functions of automatic temperature control of thermostats, flow rates and pressure of the carrier gas (EUPG system), auxiliary gases, automatic ignition of detectors, flame burning control during operation, measurement of detector signals using Gorenje 24-bit ADC. Technical specifications: The detection limit of PID is 1,1x10-12 gS/s for h-hydrocarbons 1,1x10-12 gS/s for propane. The detection limit of DTP1.7x10-14 g/s for lindane 3.9x10`15 g/s for lindane (micro-ED) The detection limit of EZD1x10`13 grus for phosphorus in metaphos 8x10`13 g5/s for sulfur in metaphos or hydrogen sulfide PFD detection limit 1.5x10`14 g/s for phosphorus in metaphos 3x10`13 GM/s for nitrogen in azobenzene Detection limit of TID2x10`10 g/ml by hydrogen The detection limit of TcD is 5x10`13 g/s for benzene The detection limit of the FEED is 3x10`13 g/s for carbon in methane 3x10`13 g/s for carbon in methane Detection limit GID500:1 (M7-801) with the introduction of 1x10`12 g / ml of octafluoroaphthalene The signal-to-noise ratio of MSD 1500:1 (Maestro-oMS) when entering 1x10`12 g / ml of octafluoroaphthalene Linear dynamic range of PID x1*107 Linear dynamic range DTP1*108 The volume of the column thermostat is 14 (19)l The temperature of the column Current.Wednesday +3 °C to +400 °C (by special order up to 450 °C) (by special order from -10°C with use. cold. ust-ki)(by special order from -100 °C. with use. liquid, no.) The discreteness of the temperature setting is 0, ° C Temperature stability 0.01 °C Temperature programming speed 0t 0.1 to 125 °C/min (by special order up to 150 °C/min) The number of isotherms is not less than 30 The cooling rate of the column thermostat is from 400 to 50 °C3.3 min. The maximum temperature of the detector and evaporator is 450 °C Carrier gas consumption from 0 to 100 ml/min.(by special order up to 500 ml/min.) Carrier gas pressure (for capillary column) from 0 to 0.40 Mpa (by special order up to 1 MPa) The maximum inlet gas pressure on a special order is 0.5 MPA 1.25 MPA Hydrogen consumption 0-500 Air consumption 0-1000 Overall dimensions (width x depth x height) 550%500*500 mm Weight 39 kg Electric power supply from AC mains voltage (220.2) V, frequency (50 +1) Hz The maximum power consumption (in steady-state mode) is 900 VA.

An automated installation for determining the wear of various catalysts, including KPS (FCC) for cracking with a fluidized bed by an air jet and is designed to determine the comparative wear characteristics of the KPS (FCC) of the catalyst by friction of an air jet according to ASTM D5757-11. It is used for testing with irregularly shaped spherical sludge particles (size from 10 to 180 microns). Abrasion is achieved by fluidization of the sample under the influence of jets of moist air. The percentage of fine particles (less than 20 microns in size) after a 5-hour test is an air jet abrasion index (AJI). technical specifications The range of operating air pressures for the power supply of the installation is 0.8±0.1 MPa The range of air flow rates for the power supply of the installation is not less than (l/min) 20 Absolute error of the air flow rate maintained automatically at a flow rate of 10 l/min. no more, l/min. ± 0.05 Power consumption not more than 0.2 kW Overall dimensions, mm and weight kg. 560x760x1700, 30 Abrasion pipe made of steel 12x18 n10t with dimensions, mm 710±10, 35 ± 0.5 Three sapphire nozzles with a diameter and length, mm 0.381±0.005, 2±1.0 Continuous operation mode Control: microprocessor with tactile control for setting the display and automatic maintenance of installation parameters and mathematical processing of analysis results 60 The convergence of the results when testing the same catalyst is not more than 0.1%

The Meta-chrome digital gas flow meter is designed to maintain a given pressure and the ratio of the amount of gases (in the flow mode) or gas flow (in the intake mode) in vacuum installations with automatic and manual control. technical specifications The number of control channels is 2 (or more on request). The maximum flow rate for each of the channels is 700 cm3/min. The possibility of using gas correction coefficients, the most commonly used gases are listed in the leaker database. The accuracy of maintaining a given proportion of gases is 5%. The accuracy of maintaining the specified gas flow rates is 3%. Input pressures from 1 to 4 atm. Electric power supply from a single—phase AC network with voltage from 187 to 242 V, frequency (50 ± 1) Hz, operating mode - continuous. Power consumption (without a personal computer), no more than — 30 VA. Overall dimensions (width × depth × height), no more than 165×350×215 mm. Weight, not more than 5.5 kg.

The dispenser "DAZH 4000" is designed for automatic insertion of liquid samples into the evaporator of the gas chromatograph, provides: control from the software, setting variable parameters of algorithms for washing and sample entry, storing the operating parameters of the dispenser in the method. Technical characteristics: The number of vials in the carousel, pcs up to 30 The volume of installed vials, ml 0.1-2ml Number of injections from one vial 1-99 Replaceable syringes in volume, ml 10, 100, 250, 500 The volume of the injected sample, ml : from 0.01 to 500 The discreteness of setting the sample volume, µl: from 0.01 to 1 Sampling and insertion rate, µl/s: from 0.01 to 5000 The speed of needle insertion into the evaporator, discret 3 Immersion depth in the vial and evaporator, variable up to the length of the syringe needle, mm 1 – 99 The discreteness of the dive depth setting, mm 0,1 The number of pumping during sampling 0-15 Number of solvent washes 0-15 Needle exposure time in the evaporator, sec 0-99 The discreteness of setting the needle shutter speed, sec 1,0 Sample input modes Simple insertion, Sandwich, Solvent sandwich, Sandwich with internal standard Flushing mode From the vial Supply voltage, V (frequency, Hz) 220 (50) Power consumption, W 154 Weight, kg, no more 2,9 Overall dimensions, mm 175x270x420 Communication with the computer Ethernet

The bench laboratory unit is designed to test the adsorption properties of silica gels, protective layers and selective hydrogenation catalysts. Ambient temperature from +10 to +35C; The relative humidity of the air is not more than 80% at a temperature of 25C;. Power supply – three- or single-phase AC network with a voltage of 220 V ± 10% with a frequency of 50 Hz.; air 0.4 — 0.8 Mpa. The average service life of the installation is 5 years. TECHNICAL CHARACTERISTICS Operating pressure range, MPa 0÷6 Reactor operating temperature range, 0C 20÷600 Reactor inner diameter, mm 20 Internal length of the reactor, mm 690 A thermocouple pocket with a movable filter and a support grid fixed on it to regulate the volume of the tested catalyst. Length of the isothermal zone, mm 300 The type of furnace is Casement Number of thermostatically controlled independent zones 4 The power consumed by each of the four independent thermostatic zones, W ≤ 400 The discreteness of the temperature setting, 0C 0.1 Flow range C2 H4, l/min 0,02÷1,7 Flow range C3 H6, l/min 0,02÷1,7 Flow range H2, l/min 0÷0.02 Flow range N2, ml/min 0.02÷1.7 Actuation pressure of mechanical safety valves, 6,8 MPa Supply voltage 220V 50Hz Power consumption not more than, kW 5 The discreteness of the temperatures and flow rates displayed on the displays is 0.01 Installation weight, kg 230 Overall dimensions of the installation, mm 1680x1480x580 Length of supply gas pipelines, m 20

The laboratory unit is designed to evaluate the activity of heterogeneous catalysts in a reactor with a fixed bed for the hydrotreating process. Ambient temperature from +10 to +35C; The relative humidity of the air is not more than 80% at a temperature of 25C;. Single-phase AC network with a voltage of 220 V ± 10% with a frequency of 50 Hz The average service life of the installation is 5 years. TECHNICAL CHARACTERISTICS OF THE HYDROTREATING AND HYDROGENATION UNIT Reactor: 1 piece Reactor volume, 240 ml Material 12X18H10T Inner diameter, mm 24 Length, mm 500 Operating temperature range, 0C 20÷600 Operating pressure range, MPa 0÷10 Removable pocket for thermocouples,mm 600 Reactor furnace: 1 piece Type of furnace Type of furnace Casement Number of thermostatic zones, pcs 3 The length of the full heated zone of the furnace, mm 450 The length of each of the four thermostatic zones, mm 150 The length of the isothermal zone of the furnace, mm 300 The power consumed by each isothermal zone, W 800 Power consumed by all three zones of the furnace, W 2400 The discreteness of the temperature setting, 0C 1 Hydrogen flow rate shaper: 1 piece Type of shaper, RGE Bronkhost Range of supported expenses, l/h 0-100 Inlet pressure, 100 bar Nitrogen flow rate shaper: 1 piece The type of the shaper, the leak (Nat2) Hy-Lok Range of supported expenses, l/h 0-10 Inlet pressure, 0-100 bar Raw material consumption shaper: 1 piece Shaper type, liquid pump KAPPA 10 Supported flow range, ml/min 0-10 Output pressure, 0-400 bar Raw material capacity: 1 piece Volume, l 4 Maximum pressure, atm 4 Working pressure, atm 0.2-1 Raw Materials Oil Installation: 1 piece Operating cycle of the installation, h 120 Inlet gas pressure calculated H2, N2, MPa 10 Actuation pressure of mechanical safety valves, 9.9 MPa Supply voltage 220V 50Hz The power consumption of the entire installation is not more than, kW 3 Installation weight without cabinet, kg 120 Overall dimensions, mm 1800x865x550 Overall dimensions of the cabinet, mm 2000x800x880

The hydrogen generator is equipped with its own microprocessor, with which you can control the operating modes of the device. It is microprocessor control that determines the autonomy of the device. Moreover, this allows you to control the basic and technical parameters of the device (pressure, flow rate, level of water poured into the tank, tightness of gas lines, electrolyzer current). For the manufacture of gas lines, exclusively inert materials are used. Technical specifications:

The device is equipped with a four-button keyboard, which is used to set parameters and control. The generator can operate in continuous mode for a long time. For refueling, especially pure or double-distilled water is used, and refueling can be done without turning off the device, on the go. Their advantage is that they significantly reduce, or even completely eliminate, the use of bottled gases to power chromatographs and gas analyzers. For nutrition, mainly double-distilled water is used, the quality of which must be no lower than grade B water according to OST 11.029.003–80, and the electrical resistivity must be no less than 1 Mohm x cm.

The devices operate from a single-phase AC electrical network with voltage from 187 to 242 W, frequency (50±1) Hz. Maximum safety of devices is achieved due to the absence of such a supply of substance in them, which could fill a chromatograph or laboratory in a short period of time. The performance of the device eliminates the occurrence of explosive situations, so the generator is considered safe to use.

The metering valve for the analysis of liquefied gas (KDSG) is designed for the introduction of liquefied gas or other liquid under excessive pressure into the evaporator of the chromatograph. KDSG is a 4-way crane, in which a dose of a certain volume is installed. The tap is installed on the evaporator of the chromatograph. A dose of any volume can be installed on the tap. Dose change can be performed by the operator. The amount of the dose volume is indicated on the tag. Technical specifications The dose volume is from 0.25 to 4.0 µl (at the request of the consumer, the dose volume can be increased up to 10 µl). The tap temperature is no more than 150 °C. The pressure in the crane line is not more than 0.48 MPa. The angle of rotation of the crane handle is 90 °C.

Tube-type thermostats and accessories for laboratory reactor installations complete with a tripod. technical specifications The operating temperature range of the thermostat is 30÷650 °C. The relative accuracy of maintaining the temperature of the thermostat is ± 0.1 ° C. The presence of an indication of the temperature set and maintained in the thermostat. The presence of a thermocouple for temperature control inside the reactor with temperature indication. The diameter and length of the tubular furnace are agreed upon when ordering. The material of the heated part of the tubular furnace (ceramic or stainless steel) is agreed upon when ordering. The height and diameter of the rack (25 or 50 mm) of the thermostat tripod are agreed upon when ordering. The height of the thermostat relative to the base is adjusted by moving on a tripod. The thermostat rotates 360° with locking for operation at any angle from vertical to horizontal. Temperature maintenance modes are isothermal or with temperature programming (multi-stage). A variant of the thermostat is proposed, consisting of two parts that open in the form of a book, each of which has its own thermostat. A variant of the thermostat with multi-zone (along the axis of the thermostat) heating and separate temperature control of each zone is proposed. A variant of a thermostat with control (control) by a personal computer (interface by agreement) is proposed. Reactors for any pressure made of steel 12X18N10T, hasteloy, titanium are offered. Condensers (refrigerators) of the product with any cooling are offered, including on "Peltier" elements. Thermostatic mixers of any type are offered for the reactor plant. Liquid pumps and gas flow shapers are offered for any expenses, gases and pressures.

To determine small concentrations of substances, in some cases it is impossible to do without their concentration in special traps. An example of the need for such concentration is the determination of impurities in permanent gases (Ne, He, H2, Ar, O2, N2, Kr, Xe), the concentration of impurities is less than 1 ppm. Considering that these impurities can be not only hydrocarbons, but also permanent gases themselves, the use of direct detection of impurities by a catarometer is impossible. It is also not always possible to use highly sensitive but expensive detectors (GID, EDD, etc.). TECHNICAL CHARACTERISTICS The volume of the trap is 5 ml. The volume of the Dewar vessel (serial metal thermos) is 1200 ml. The concentration temperature range is from minus 88.6 (ethane) to minus 269 °C (helium). The ability to calibrate the chromatograph from the cylinder without disturbing the gas circuit. The possibility, simultaneously with concentration, to purify the gas intended for purging the trap from impurities (in a similar trap). Overall dimensions, no more than — 290 ×470 × 615 mm. Weight, not more than — 8 kg.

The pyrolytic gas chromatography method is widely used in the study of polymer materials, plastics, rubbers, rubbers, paints and other high-molecular compounds of natural and artificial origin. The method is based on thermal decomposition of sample samples in an inert medium (without oxygen access), followed by chromatographic separation and analysis of the formed volatile compounds. Thus, the resulting pyrogram allows us to judge the composition of the original sample. Pyrolysis is also used in geochemical studies. Technical specifications The volume of the capsule is 56 ml. Pyrolysis temperature — from 200 to 1000 °C. The error of maintaining the temperature is not more than 1.0 ° C. The heating time of the sample to the pyrolysis temperature is no more than 2 seconds. The cooling time of the capsule when moving from the hot zone to the cold zone after pyrolysis is no more than 10 seconds. The time of continuous operation in the pyrolysis mode is no more than 60 seconds. Electric power supply from the AC network with voltage (220index) V, frequency (50 ± 1) Hz. Power consumption — no more than 100 VA. Overall dimensions of the control unit (width ×depth×height) — 210×190×100 mm. Overall dimensions of the input node (width× depth×height) — 90×135×160 mm. The weight of the control unit is not more than 2.5 kg. The weight of the input node is not more than 0.9 kg.