Automated portable chromatograph FGH

The PCU-1 laboratory catalytic unit is designed to perform the following tasks: 1. Educational and scientific research of chemical processes; 2. Improvement of current industrial processes and development of new ones; 3. Studies of homogeneous and heterogeneous catalysts. The PCU-1 laboratory catalytic unit is manufactured in accordance with the technical requirements of customers so as to correspond to a wide range of technological parameters. Additionally, embedded equipment is designed to control the flow of raw materials and products, as well as data collection and processing. The unit can be subsequently modernized for new purposes. Main advantages: 1. A reliable and high-precision system of control and regulation of technological parameters; 2. Easy replacement of catalyst samples; 3. The possibility of conducting long-term tests in continuous mode; 4. The possibility of upgrading the unit for new purposes; 5. The possibility of conducting tests in flow and flow-circulation modes; 6. Control and accurate reproduction.

The FGH-1-2 chromatographs have retained the main advantages of the FGH-1 model – mobility and ease of operation and maintenance. At the same time, FGH-1-2 has all the advantages of a modern multichannel chromatograph – the ability to reliably identify and accurately determine the concentrations of various pollutants of environmental objects. The additional use of automatic identification in the processing of chromatograms simultaneously through both channels makes FGH-1-2, in fact, a universal selective gas analyzer of organic substances using the chromatographic separation method. In FGH-1-2, as well as in FGH-1, all methodological problems have been solved: all measurement methods (MI) used are certified, the devices are equipped with sampling devices prescribed in MI, the devices are graded according to the required substances, independent control of the stability of calibration characteristics and measurement errors is provided.

The gas chromatograph "Kristallux-4000M" is fully automated, starting from sample input and ending with chromatographic information processing, including the functions of automatic temperature control of thermostats, flow rates and pressure of the carrier gas (EUPG system), auxiliary gases, automatic ignition of detectors, flame burning control during operation, measurement of detector signals using Gorenje 24-bit ADC. Technical specifications: The detection limit of PID is 1,1x10-12 gS/s for h-hydrocarbons 1,1x10-12 gS/s for propane. The detection limit of DTP1.7x10-14 g/s for lindane 3.9x10`15 g/s for lindane (micro-ED) The detection limit of EZD1x10`13 grus for phosphorus in metaphos 8x10`13 g5/s for sulfur in metaphos or hydrogen sulfide PFD detection limit 1.5x10`14 g/s for phosphorus in metaphos 3x10`13 GM/s for nitrogen in azobenzene Detection limit of TID2x10`10 g/ml by hydrogen The detection limit of TcD is 5x10`13 g/s for benzene The detection limit of the FEED is 3x10`13 g/s for carbon in methane 3x10`13 g/s for carbon in methane Detection limit GID500:1 (M7-801) with the introduction of 1x10`12 g / ml of octafluoroaphthalene The signal-to-noise ratio of MSD 1500:1 (Maestro-oMS) when entering 1x10`12 g / ml of octafluoroaphthalene Linear dynamic range of PID x1*107 Linear dynamic range DTP1*108 The volume of the column thermostat is 14 (19)l The temperature of the column Current.Wednesday +3 °C to +400 °C (by special order up to 450 °C) (by special order from -10°C with use. cold. ust-ki)(by special order from -100 °C. with use. liquid, no.) The discreteness of the temperature setting is 0, ° C Temperature stability 0.01 °C Temperature programming speed 0t 0.1 to 125 °C/min (by special order up to 150 °C/min) The number of isotherms is not less than 30 The cooling rate of the column thermostat is from 400 to 50 °C3.3 min. The maximum temperature of the detector and evaporator is 450 °C Carrier gas consumption from 0 to 100 ml/min.(by special order up to 500 ml/min.) Carrier gas pressure (for capillary column) from 0 to 0.40 Mpa (by special order up to 1 MPa) The maximum inlet gas pressure on a special order is 0.5 MPA 1.25 MPA Hydrogen consumption 0-500 Air consumption 0-1000 Overall dimensions (width x depth x height) 550%500*500 mm Weight 39 kg Electric power supply from AC mains voltage (220.2) V, frequency (50 +1) Hz The maximum power consumption (in steady-state mode) is 900 VA.

Overall dimensions: 550x230x350 mm Weight (without computer): ~17 kg Power consumption: up to 200 watts Warranty service : 1 year   Detector Two-beam spectrophotometer Spectral range – 190-360 nm Simultaneous detection at 1-8 wavelengths Cell volume – 1.2 µl Noise <0.0001 E.O.P. at 250 nm Drift <0.00005 E.O.P./hour at 250 nm Column Ø2x75 mm stainless steel The efficiency of the column is up to 6000 theoretical plates Thermostat Solid-state electric Set temperature from 35 to 90°C The discreteness of the temperature setting is 1 °C Temperature control error ±0.3°C      Pump Two-pronged, gradient The feed rate is from 5 to 1000 µl/min, the maximum pressure is 70 atm . The gradient is formed from 1 to 20 linear sections Automatic doser Automatic, programmable Number of test tubes – 46 The number of analyses in the series is from 1 to 200 The dosed volume is from 1 to 99 µl Test tubes made of glass with a volume of 200 µl Polyethylene tube stoppers Software OS: Windows® XP/7/10 Milichrome A-02™, Multichrome™, Alphachrome, Alphaspectrum

Technical characteristics: DETECTOR - TYPE OF CHROMATOGRAPH - DETECTION LIMIT, G/S (G/ML) -STANDARD DEVIATION, % - LEVEL OF FLUCTUATIONAL NOISES, A (V) -DRIFT, А/H (V/H) FID Crystall-2000 5×10⁻¹² 2 2×10⁻¹⁴ 4×10 ⁻¹³ TCD Crystall-2000 (5×10⁻⁹) 2 (2×10⁻⁷) (2×10⁻⁵) ADC Crystall-2000 5×10⁻¹⁴ 4 1×10⁻¹² 8×10⁻¹¹ FPD-Р Crystall-2000 2×10⁻¹² 6 2×10⁻¹¹ 4×10⁻¹⁰ FPD-S Crystall-2000 2×10⁻¹¹ 10 2×10⁻¹¹ 4×10⁻¹⁰

The compounds to be determined are marginal and unsaturated hydrocarbons, alcohols, esters and esters, aromatic hydrocarbons, ketones, petroleum products, solvents, chlorine derivatives of hydrocarbons, etc. The list of substances is constantly updated, currently includes more than 100 ingredients. Detector one photoionization detector (PID) with Krypton vacuum ultraviolet lamp (VUV) One capillary column 25 m, phase SE, OB-61, FFAP, 624, etc. The threshold for determining benzene in air is 0.01 mg/m3 Average analysis time 15 min Powered by built-in batteries, 220 V mains Dimensions 460×350×120 mm (standard case), 487×370×180 (shockproof case) Autonomy of up to 300 analyses without replacement of carrier gas, up to 5 hours without charging batteries (for chromatograph without heated dispenser tap) Metrology Portable gas chromatographs of the FGH series, in particular the FGH-1 model, are registered in the State Register of Measuring Instruments under No. 16615-07 (certificate RU.C.31.004.A No.30175/1 dated 12/26/2012). All methods of analysis are certified in accordance with GOST R ISO 5725-6 and entered into the Federal Register.

Technical specifications: Operating spectral range, nm from 190 to 360 Limits of permissible absolute error of wavelength setting, nm ± 5 Detection limit of anthracene (wavelength 252 nm), ng/cm3, no more than 1 The limit of the permissible value of the relative mean square deviation of the output signal (n =5), % of the retention time over the peak area of 1.5 2 Limits of the permissible value of the relative change in the output signal (peak area) for 4 hours of continuous operation, % ± 5 Overall dimensions (LxWxH), mm, no more: 270x420x190 Weight, kg, not more than 9.5 Power consumption, V· A, not more than 50

The liquid chromatograph "Lumachrom-M" provides maximum automation of the analysis. The device is controlled using specialized software, which in combination with the continuous eluent supply mode and the autosampler gives the maximum level of autonomy of operation. In addition, such a solution minimizes labor costs and the influence of the human factor. The unique design solutions of the chromatograph provide continuous pulsation-free flow of the mobile phase in both isocratic and gradient modes, as well as the ability to work with any column sizes. Thanks to the improved technical characteristics on the Lumachrom-M device, it is possible to implement a wider list of techniques and GOST compared to previous models.

We offer expert laboratories of physicochemical methods of analysis a gas chromatograph with a quadrupole mass spectrometric detector «MAESTRO-αMS». Quadrupole GC-MS «MAESTRO-αMS» is in demand for targeted research (screening) and non-targeted search. In targeted studies, it is necessary to detect given target compounds in samples of various nature and origin at the level of residual amounts, for example, several picograms of the target compound in the injected 1 μl of liquid sample. Most often, targeted research is carried out in the following areas of laboratory screening: ecology, food safety, clinical monitoring, narcology, doping control, production control of various raw materials. In targeted studies, it is often required not only to confirm the presence of a compound in a sample, but also to determine the level of its content quantitatively, since both the list of target compounds and the permissible level of their presence in the sample are specified by regulatory documents. Quantitative analysis requires standards for the substances you are looking for. When conducting a non-target search, as a rule, it is required to analyze a sample of unknown composition, in other words, to find as many compounds as possible in the sample and identify (identify) each of them. Since the identification of a detected compound is carried out by comparing its experimental mass spectrum with the spectrum of a pure substance obtained under standard conditions, this task requires reference libraries of mass spectra of pure substances, as well as tools for working with mass spectra, for example: algorithms for cleaning experimental mass spectra from background and spectral noise (mass spectrum deconvolution algorithms), library search and comparison algorithms. An off-target search is called a qualitative analysis, since the researcher is primarily interested in the list of detected substances, and not in the quantitative assessment of their content in the sample. When creating MAESTRO-αMS, we took into account our own many years of experience in operating imported analogues. We have made the device inexpensive. We have made the device compact: The modern design of the device made it possible to make the MAESTRO-αMS really compact, so that the device occupies the smallest possible area on the laboratory table. The layout of the device allows you to remove the ion source on the front flange for cleaning and replacing the cathodes, if necessary. We have reduced the cost of operation: When developing the MAESTRO-αMS, we sought to increase the resistance of the device to sample matrices and use a minimum of consumable materials in order to eliminate downtime for maintenance and replacement. As a result, we have created an extremely stable ion source and a perpetual photomultiplier detector. We have created special software: Even at the first acquaintance with the software, it becomes obvious that being in the window of each button and each parameter to be changed is expedient and logical. Our software product was created for the convenience of the operator, so we implemented the necessary and eliminated the unnecessary. We used the principle of one active window, in which the operator moves sequentially step by step, performing hardware settings, setting the data collection method, subsequent processing algorithms, templates for presenting the results. MAESTRO-αMS offers a wide range of scanning modes, built-in algorithms for working with mass spectral data, convenient unloading of initial data arrays for their processing in specialized software packages, graphics export for presentations and scientific publications. You can use several libraries of mass spectra at the same time, or create your own for your typical tasks. Finally, we provide a 5-day training course for professionals who want to understand the theoretical foundations of the method and their implementation in the hardware of modern quadrupole GC/MS. The volume and depth of presentation of the material from the developers of the device is intended to lay the foundation for the effective use of «MAESTRO-αMS» in the future. Some technical characteristics of MAESTRO-αMS: • Instrumental detection limit (SIM, OFN @272 m/z ) < 10 fg; • Scan modes: scan for selected ions, full scan in a given mass range, combined scan mode; • The number of simultaneously connected libraries of mass spectra is at least 10.