Energy dispersive sulfur-in-oil analyzer ASE-2

It is designed for recording absorption spectra of solid, liquid and gaseous substances in the near and middle IR region (including drugs, lacquers and paints, petroleum products, explosives, pharmacological preparations, polymer films and fibers) with their subsequent identification, as well as for qualitative and quantitative analysis of mixtures containing several components.

When analyzing gases dissolved in transformer oil using the ARP method (equilibrium vapor analysis), mixing of the contents of the syringe with oil is used to accelerate the extraction of gases (to achieve an equilibrium distribution of gases dissolved in oil between the liquid and gas phases). For this purpose, as well as automation of the mixing process, a special autonomous device for achieving equilibrium is produced. technical specifications The rotation speed of the syringe drum is 30 rpm./min. The rotation time (determined by the internal timer, after pressing the "Start" button) is 10 minutes. The number of syringes placed is 4. The volume of syringes is 20 or 50 ml. Power consumption, no more than — 14 VA. Overall dimensions, no more than 210×280×270 mm. Weight, not more than — 5 kg.

To analyze small concentrations of carbon monoxide (CO) and carbon dioxide (CO2), instead of the usual catarometer for these gases, a more sensitive PID is used, while carbon oxides are converted into methane (CH4) using reaction chromatography. The device implementing the conversion reaction is called a methanator, i.e. a device with a special catalyst that converts CO, CO2 into methane in a hydrogen current, while the latter is either a carrier gas itself, or is blown together with the carrier gas into the methanator through a tee. The methanator provides a highly efficient conversion reaction, while the detection limit of carbon oxides reaches 0.1 ppm. technical specifications Metanation temperature — 330 °C The coefficient of metanation is not less than 95 % The effective volume of the methanator is 1 ml.

The device is designed to extract target organic substances from liquid and solid samples. Implements the latest method of sample preparation in chemical analysis - extraction freezing with centrifugation of EVCB (Patents of the Russian Federation RU2303476/2007, RU2564999/2015, Patent of the Kyrgyz Republic KG388/2020, International Application PCT/RU2015/000615). Scope of application - hydrochemistry, chemical and toxicological analysis, biochemistry, food research, etc. technical specifications The temperature range of extraction freezing with centrifugation is from -(minus) 28 to +25 °C. Rotor speed with the possibility of programming the mode 100-8000 rpm Separation factor up to 6600 g Cryoextractor power supply from AC 220 V, 50 Hz Power consumption, not more than 0.3 kW The mass of the cryoextractor is not more than 50 kg Overall dimensions (HxWxD), mmxmmxmm no more than 900x600x600 Number of simultaneously extracted samples (individually on request)

Technical specifications: ESI / APCI ionization method Time-of-Flight Mass Analyzer The maximum repetition frequency of the ejection pulses is 10 kHz Recording speed of spectra Up to 100 spectra per second Characteristics of a 12-bit ADC, 2 GHz The number of simultaneously defined components is unlimited Mass range 1-2000 m/z Resolution > 4000 Vacuum system of 2 Fornaps and 3 TMN (240 l/sec) Overall dimensions 1450×780×1550 mm

Technical specifications: Method of ionization Plasma pulsed glow discharge Discharge gas Argon, consumption less than 1 l/hour Time-of-flight Mass Analyzer with mesh-free ion mirror Resolution 4000 The number of simultaneously defined components is unlimited Mass range 1-1000 m/z Detection limits 1-100 ppb Layer-by-layer resolution Up to 5 nm Depth of analysis Up to 30 microns The time for one analysis of a solid sample is 30 minutes (with the option of a revolver system – 3-5 minutes) Vacuum system 1 Booster pump and 2 TMN (240 l/sec) Overall dimensions 1450×780×1550 mm

Technical specifications: Measuring range 0.5–500 ng Sample dispenser capacity 5000 mg / 2800 ml Analysis time 1-5 min Operating temperature range with software control 50-950 °C with software control The capacity of the autosampler is 45 samples Power supply 220 ± 22 V, 50 ± 1 Hz Dimensions (LxWxH), no more: with autosampler without autosampler 450x840x460 mm 450x490x460 mm Weight, no more: with autosampler without autosampler 57 kg 40 kg

Technical specifications: The upper limit of the measurement range is 5 mg/kg Analysis time 1-5 min Permissible sample weights are 10-500 mg The weight of the console is 17 kg Air pumping speed 1-3 l/min Dimensions and weight of the analyzer 470x210x110 mm; 7.5 kg Power supply of the PIRO-915+ 220 V, 700 W Analyzer power supply 220 V, 15 W Dimensions of the power supply and pumping unit no more than 400x280x135 mm The dimensions of the thermal camera unit and the remote optical unit are no more than 430x340x135 mm The upper limit of the measurement range for sample weighting is 20 mg 200 mg/kg

It can be used as a primary source of carrier gas, since it is equipped with an additional gas purification system. This device is especially relevant when, for some reason, helium is not available to the consumer (for example, when working with a thermal conductivity detector - an accident). Due to the high thermal conductivity of hydrogen, TTP operates with significantly greater sensitivity than helium.

The gas chromatograph "Kristallux-4000M" is fully automated, starting from sample input and ending with chromatographic information processing, including the functions of automatic temperature control of thermostats, flow rates and pressure of the carrier gas (EUPG system), auxiliary gases, automatic ignition of detectors, flame burning control during operation, measurement of detector signals using Gorenje 24-bit ADC. Technical specifications: The detection limit of PID is 1,1x10-12 gS/s for h-hydrocarbons 1,1x10-12 gS/s for propane. The detection limit of DTP1.7x10-14 g/s for lindane 3.9x10`15 g/s for lindane (micro-ED) The detection limit of EZD1x10`13 grus for phosphorus in metaphos 8x10`13 g5/s for sulfur in metaphos or hydrogen sulfide PFD detection limit 1.5x10`14 g/s for phosphorus in metaphos 3x10`13 GM/s for nitrogen in azobenzene Detection limit of TID2x10`10 g/ml by hydrogen The detection limit of TcD is 5x10`13 g/s for benzene The detection limit of the FEED is 3x10`13 g/s for carbon in methane 3x10`13 g/s for carbon in methane Detection limit GID500:1 (M7-801) with the introduction of 1x10`12 g / ml of octafluoroaphthalene The signal-to-noise ratio of MSD 1500:1 (Maestro-oMS) when entering 1x10`12 g / ml of octafluoroaphthalene Linear dynamic range of PID x1*107 Linear dynamic range DTP1*108 The volume of the column thermostat is 14 (19)l The temperature of the column Current.Wednesday +3 °C to +400 °C (by special order up to 450 °C) (by special order from -10°C with use. cold. ust-ki)(by special order from -100 °C. with use. liquid, no.) The discreteness of the temperature setting is 0, ° C Temperature stability 0.01 °C Temperature programming speed 0t 0.1 to 125 °C/min (by special order up to 150 °C/min) The number of isotherms is not less than 30 The cooling rate of the column thermostat is from 400 to 50 °C3.3 min. The maximum temperature of the detector and evaporator is 450 °C Carrier gas consumption from 0 to 100 ml/min.(by special order up to 500 ml/min.) Carrier gas pressure (for capillary column) from 0 to 0.40 Mpa (by special order up to 1 MPa) The maximum inlet gas pressure on a special order is 0.5 MPA 1.25 MPA Hydrogen consumption 0-500 Air consumption 0-1000 Overall dimensions (width x depth x height) 550%500*500 mm Weight 39 kg Electric power supply from AC mains voltage (220.2) V, frequency (50 +1) Hz The maximum power consumption (in steady-state mode) is 900 VA.

The pyrolytic gas chromatography method is widely used in the study of polymer materials, plastics, rubbers, rubbers, paints and other high-molecular compounds of natural and artificial origin. The method is based on thermal decomposition of sample samples in an inert medium (without oxygen access), followed by chromatographic separation and analysis of the formed volatile compounds. Thus, the resulting pyrogram allows us to judge the composition of the original sample. Pyrolysis is also used in geochemical studies. Technical specifications The volume of the capsule is 56 ml. Pyrolysis temperature — from 200 to 1000 °C. The error of maintaining the temperature is not more than 1.0 ° C. The heating time of the sample to the pyrolysis temperature is no more than 2 seconds. The cooling time of the capsule when moving from the hot zone to the cold zone after pyrolysis is no more than 10 seconds. The time of continuous operation in the pyrolysis mode is no more than 60 seconds. Electric power supply from the AC network with voltage (220index) V, frequency (50 ± 1) Hz. Power consumption — no more than 100 VA. Overall dimensions of the control unit (width ×depth×height) — 210×190×100 mm. Overall dimensions of the input node (width× depth×height) — 90×135×160 mm. The weight of the control unit is not more than 2.5 kg. The weight of the input node is not more than 0.9 kg.

The liquid chromatograph "Lumachrom-M" provides maximum automation of the analysis. The device is controlled using specialized software, which in combination with the continuous eluent supply mode and the autosampler gives the maximum level of autonomy of operation. In addition, such a solution minimizes labor costs and the influence of the human factor. The unique design solutions of the chromatograph provide continuous pulsation-free flow of the mobile phase in both isocratic and gradient modes, as well as the ability to work with any column sizes. Thanks to the improved technical characteristics on the Lumachrom-M device, it is possible to implement a wider list of techniques and GOST compared to previous models.

The dispenser "DAZH 4000" is designed for automatic insertion of liquid samples into the evaporator of the gas chromatograph, provides: control from the software, setting variable parameters of algorithms for washing and sample entry, storing the operating parameters of the dispenser in the method. Technical characteristics: The number of vials in the carousel, pcs up to 30 The volume of installed vials, ml 0.1-2ml Number of injections from one vial 1-99 Replaceable syringes in volume, ml 10, 100, 250, 500 The volume of the injected sample, ml : from 0.01 to 500 The discreteness of setting the sample volume, µl: from 0.01 to 1 Sampling and insertion rate, µl/s: from 0.01 to 5000 The speed of needle insertion into the evaporator, discret 3 Immersion depth in the vial and evaporator, variable up to the length of the syringe needle, mm 1 – 99 The discreteness of the dive depth setting, mm 0,1 The number of pumping during sampling 0-15 Number of solvent washes 0-15 Needle exposure time in the evaporator, sec 0-99 The discreteness of setting the needle shutter speed, sec 1,0 Sample input modes Simple insertion, Sandwich, Solvent sandwich, Sandwich with internal standard Flushing mode From the vial Supply voltage, V (frequency, Hz) 220 (50) Power consumption, W 154 Weight, kg, no more 2,9 Overall dimensions, mm 175x270x420 Communication with the computer Ethernet

The autosampler is used to automate the process of entering samples of liquid consistency into chromatographs of the line "Kristallux", "Crystal", series "Color", LHM. The autosampler is compact in size and easy to operate. The device is compatible with different models of chromatographs and is suitable for many studies. When the device is working with the Crystallux series chromatographs, the autosampler can be controlled using the chromatographic equipment software, while no additional programs are required.

The compounds to be determined are marginal and unsaturated hydrocarbons, alcohols, esters and esters, aromatic hydrocarbons, ketones, petroleum products, solvents, chlorine derivatives of hydrocarbons, etc. The list of substances is constantly updated, currently includes more than 100 ingredients. Detector one photoionization detector (PID) with Krypton vacuum ultraviolet lamp (VUV) One capillary column 25 m, phase SE, OB-61, FFAP, 624, etc. The threshold for determining benzene in air is 0.01 mg/m3 Average analysis time 15 min Powered by built-in batteries, 220 V mains Dimensions 460×350×120 mm (standard case), 487×370×180 (shockproof case) Autonomy of up to 300 analyses without replacement of carrier gas, up to 5 hours without charging batteries (for chromatograph without heated dispenser tap) Metrology Portable gas chromatographs of the FGH series, in particular the FGH-1 model, are registered in the State Register of Measuring Instruments under No. 16615-07 (certificate RU.C.31.004.A No.30175/1 dated 12/26/2012). All methods of analysis are certified in accordance with GOST R ISO 5725-6 and entered into the Federal Register.

Technical specifications: Ionization method Glow discharge plasma Discharge gas Air Time-of-flight Mass Analyzer with mesh-free ion mirror Resolution 4000 The number of simultaneously defined components is not limited Mass range 1-1000 m/z Detection limits 10-100 ppt Analysis time 1-3 min Vacuum system 1 Booster pump and 2 TMN (240 l/sec) Overall dimensions 1450×780×1550 mm

Technical characteristics: The set-top box is powered by AC (220 ± 22) V, 50 Hz Power consumption, VA, no more than 35 Continuous operation time, h 8 Overall dimensions: (LxWxH), mm, no more than 320x290x160 The weight of the console, kg, not more than 6.5 Air consumption, dm3/min 2 ... 5