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Atomic Emission Complex "Grand Stream" is designed for rapid determination of the composition of powder samples of natural and industrial origin, includes a "Grand" spectrometer, a "Stream" installation and auxiliary equipment for sample preparation.

It is designed for recording absorption spectra of solid, liquid and gaseous substances in the near and middle IR region (including drugs, lacquers and paints, petroleum products, explosives, pharmacological preparations, polymer films and fibers) with their subsequent identification, as well as for qualitative and quantitative analysis of mixtures containing several components.

Atomic Emission Complex "Grand Globula" includes a spectrometer "Grand", a spectroanalytic generator "Ball Lightning" and a tripod "Globula". It allows the analysis of various substances and materials in arc and spark discharges in air, for example according to GOST 17818.15-90 "Graphite. Spectral analysis method", GOST 9717.1-82 "Copper. A method of spectral analysis based on metallic standard samples with photoelectric spectrum registration" and other MVIS.

It allows recording transmission spectra of objects with sizes from 500 microns (precious stones, optical parts, semiconductor materials). It is also used in the study of samples compressed into small-diameter tablets with KBr (the method is convenient for spectral analysis of powdery substances - the prefix allows you to work with small amounts of the sample using a manual press for the manufacture of tablets). • The diameter of the focus spot is less than 3 mm • The design uses parabolic mirror optics • The set-top box is equipped with a set of replaceable diaphragm holders for samples of different sizes • Windows-substrates made of IR-transparent materials can be placed in the holder after pasty, liquid substances or extracts are applied to them, followed by drying of the layers • The slide table has the possibility of smooth movement in vertical and horizontal directions to achieve the maximum signal level

The installation is designed to excite atomic emission spectra of powder samples in an electric arc by the spillage-injection method. It provides high performance of routine analyses, has a low consumption of graphite electrodes and is used in conjunction with any spectral devices – "Grand", STE-1, DFS-458, MFS-8, PGS-2, etc.

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To achieve the maximum sensitivity during measurements, a special prefix is used to the FT-801 Fourier spectrometer, which is an optical unit with a built-in highly sensitive MST detector cooled with liquid nitrogen. The set-top box is installed in the cuvette compartment of the spectrometer and connected to the corresponding external electrical port, the detector is turned on programmatically. In this case, the sensitivity of the method increases many times (up to 20) – depending on the type of standard uncooled detector in the spectrometer). The speed of recording spectra is also increasing. The operating time after filling the cryostat (200 ml capacity) with liquid nitrogen is at least 6 hours. Increasing the sensitivity of the spectrometer using a prefix with an MST detector may be required for many applications: in fiber spectroscopy, when recording emission spectra of low-power emitters, in trace gas analysis with high spectral resolution, when determining the presence of impurities in samples in ultra-low concentrations, when using multi-pass gas cuvettes, etc. In the picture: on the left in the cuvette compartment there is a capler with fiber from Art photonics GmbH, Berlin, Germany, on the right there is a prefix with an MST detector. Technical specifications The recommended number of scans when registering spectra is 16 Spectrum registration time at 50 scans (resolution 4 cm-1), sec 20 Cryostat capacity, 200 ml Working time after filling the cryostat, 6 hours Overall dimensions, mm 225×175×75 Weight, kg 1.45

The main difference between this set-top box and the universal set-top box of the NPVO and ZDO is that a prism is used as a working element of the MNPVO, which allows to obtain several reflections from the area of contact with the sample under study, which leads to an improvement in the quality of the spectrum and an increase in the sensitivity of the method (absorption bands become more pronounced). The registration of specular and diffuse reflection spectra (ZDO) is not provided on this set-top box. The MNPVO prefix is effective in registering the absorption spectra of samples whose dimensions (number) are sufficient to ensure contact with the entire area of the working face of the prism: * liquids of any degree of viscosity (solutions, suspensions, oils, etc.); * solid elastic samples (polymer fragments of sufficiently large size, rubbers, plastics, etc.); * powdered samples in quantities sufficient to be applied to the entire surface and samples in the form of thin tapes; The universal clamp is equipped with a precision lever mechanism for quickly lowering the tip and a micrometer screw that allows you to pre–set the optimal degree of pressure - this ensures quick sample change and repeatability of the results during measurements. For convenience when working with liquid and paste-like samples, it is possible to rotate the clamping console by 180o. Note: the MNPVO prefix does not exclude the possibility of registering the spectra of samples whose dimensions are smaller than the area of the working face of the prism (the presence of a visual inspection system of the surface under study increases convenience when working with small-sized objects), but the overall effectiveness of the method is significantly lower than when using the universal NPVO and ZDO prefix. Transmission in the operating range of the spectrum, % of the input signal of at least 25 · The recommended number of scans when registering spectra is 25 · Spectrum registration time at 25 scans (resolution 4 cm-1), 30 seconds · The depth of penetration of radiation into the sample, microns 5 – 15 · Minimum area of a solid sample, mm2 1 · Minimum volume of the test liquid, ml 0.3 · The permissible pH range of the analyzed objects is from 5 to 9 · Crystal substrate material ZnSe CVD, Ge · Diameter of the focus spot, mm 3 · Number of reflections 3 · The size of the working face of the prism, mm 21 X 6 · Magnification of the 4X micro lens · Total magnification of the visual channel 75X · Field of view of the optical system, mm 2 X 2.5 · Digital video camera resolution 640 X 480 · Overall dimensions, mm 145×125×240 · Weight, kg 2

It is used for recording transmission spectra of medium–sized and arbitrary-shaped solid samples - polymer films of various thicknesses, optical parts, semiconductor wafers, large crystals, etc. • Thanks to quick-release nuts, it provides convenient fastening of samples

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Overall dimensions: 550x230x350 mm Weight (without computer): ~17 kg Power consumption: up to 200 watts Warranty service : 1 year   Detector Two-beam spectrophotometer Spectral range – 190-360 nm Simultaneous detection at 1-8 wavelengths Cell volume – 1.2 µl Noise <0.0001 E.O.P. at 250 nm Drift <0.00005 E.O.P./hour at 250 nm Column Ø2x75 mm stainless steel The efficiency of the column is up to 6000 theoretical plates Thermostat Solid-state electric Set temperature from 35 to 90°C The discreteness of the temperature setting is 1 °C Temperature control error ±0.3°C      Pump Two-pronged, gradient The feed rate is from 5 to 1000 µl/min, the maximum pressure is 70 atm . The gradient is formed from 1 to 20 linear sections Automatic doser Automatic, programmable Number of test tubes – 46 The number of analyses in the series is from 1 to 200 The dosed volume is from 1 to 99 µl Test tubes made of glass with a volume of 200 µl Polyethylene tube stoppers Software OS: Windows® XP/7/10 Milichrome A-02™, Multichrome™, Alphachrome, Alphaspectrum

Vacuum spectrometers are designed for rapid analysis of alloys based on iron, copper, aluminum and other metals in factory and research laboratories, including the determination of elements having analytical lines in the field of vacuum ultraviolet (VUV) (for example, S, P and C in steels).