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The autoclave is designed to simulate various chemical processes occurring at elevated temperatures and pressures. Ambient temperature from +10 to +35C; The relative humidity of the air is not more than 80% at a temperature of 25C;. Atmospheric pressure from 84 to 107 kPa (from 630 to 800 mmHg); The power supply is a single–phase AC network with a voltage of 220V ± 10% with a frequency of 50 Hz. The average service life of the autoclave is 5 years. TECHNICAL CHARACTERISTICS OF THE HYDROTREATING AND HYDROGENATION UNIT Operating pressure range, MPa 0.1-2 Reactor operating temperature range, 0C 30÷200 Autoclave flask volume, l 10 The speed control range of the agitator, rpm 20÷120 The diameter of the drain bottom valve, mm 20 Flask and lid connection flanged Power supply, single-phase network 230-240V 50-60Hz Power consumption not more than, kW 1 Overall dimensions, mm 555x1880x705 Continuous operation mode

The hardware and software complex for measuring the signals of chromatographs "Meta-chrome" (complex) is designed to automate the old fleet of chromatographs of the type LHM, model-3700, series "Color", etc. in terms of measuring the chromatographic signal and automating the processing of chromatographic information. The complex consists of two interconnected functional modules: a logarithmic digital current meter (ITLC) and a chromatographic information processing program "NetChrom" (hereinafter referred to as the processing program). technical specifications The number of analog inputs is 1. Data exchange with a personal computer — via the standard RS-232C interface. The input impedance is at least 1×106 Mohm. The range of input currents is from 1×10-14 to 5×10-7 A. The minimum measured half—width of the chromatographic peak is 0.5 s. The level of fluctuation noise brought to the input is no more than 1.2 × 10-14 A. The reduced error of the linearity of the signal conversion, no more than ± 1%. Electric power supply from a single—phase AC network with voltage from 187 to 242 V, frequency (50 ± 1) Hz, operating mode - continuous. Power consumption (without a personal computer), no more than — 3 VA. Overall dimensions (width × depth × height), not more than — 230 ×150 × 55 mm. Weight, not more than 1.3 kg.

The metering valve for the analysis of liquefied gas (KDSG) is designed for the introduction of liquefied gas or other liquid under excessive pressure into the evaporator of the chromatograph. KDSG is a 4-way crane, in which a dose of a certain volume is installed. The tap is installed on the evaporator of the chromatograph. A dose of any volume can be installed on the tap. Dose change can be performed by the operator. The amount of the dose volume is indicated on the tag. Technical specifications The dose volume is from 0.25 to 4.0 µl (at the request of the consumer, the dose volume can be increased up to 10 µl). The tap temperature is no more than 150 °C. The pressure in the crane line is not more than 0.48 MPa. The angle of rotation of the crane handle is 90 °C.

The equilibrium steam dispenser "DRP-10 (DRP-13)" is designed for the introduction of volatile components from matrices into the chromatograph, the introduction of which into the chromatograph is impossible or undesirable. Examples of such matrices are natural, drinking and waste water, soil, biological fluids, food and beverages, various polymers, building materials, pharmaceutical products, etc. The use of DRP-10 (DRP-13) makes it possible to avoid contamination of the evaporator, column and chromatograph detector with non-volatile or non-volatile substances, to avoid the consumption of solvent required for extraction, to increase the reproducibility of analyses. Technical specifications The temperature of the thermostat of containers with a breakdown is from ambient temperature to 150 °C. The error of maintaining the temperature is not more than 0.1 ° C. The volume of the container with the sample is 20 ml, it is possible to use vials from 6 to 40 ml. The number of simultaneously thermostatically controlled containers is 4. The dosed volume of the equilibrium vapor is up to 2 ml. The temperature of the syringe is from ambient temperature to 150 °C. The gas consumption for purging is from 5 to 300 ml/min. Electric power supply from the AC network with voltage (220index) V, frequency (50 ± 1) Hz. Overall dimensions (width × depth × height) — 350×270×170 mm. Power consumption — no more than 360 VA. Weight — no more than 6.5 kg.

To analyze small concentrations of carbon monoxide (CO) and carbon dioxide (CO2), instead of the usual catarometer for these gases, a more sensitive PID is used, while carbon oxides are converted into methane (CH4) using reaction chromatography. The device implementing the conversion reaction is called a methanator, i.e. a device with a special catalyst that converts CO, CO2 into methane in a hydrogen current, while the latter is either a carrier gas itself, or is blown together with the carrier gas into the methanator through a tee. The methanator provides a highly efficient conversion reaction, while the detection limit of carbon oxides reaches 0.1 ppm. technical specifications Metanation temperature — 330 °C The coefficient of metanation is not less than 95 % The effective volume of the methanator is 1 ml.

The gas flow shaper (FGP) is designed to automate the old fleet of chromatographs of the LHM type, model-3700, "Color" series, etc. in terms of setting and regulating the flow and pressure of both the carrier gas and auxiliary gases. The FGP has a flexible structure and provides regulation of gas flows from two to four independent gas flow channels and up to three pressure channels. The gas pressure at the inlet is (0.4 ± 0.04) MPa. The operating flow ranges of the carrier gas are from 3 to 250 ml/min with a discreteness of 1 ml/min. The ability to specify the type of gas (nitrogen, helium, hydrogen, argon, air). The ranges of hydrogen consumption are from 3 to 250 ml/min with a discreteness of 1 ml/min. The air flow ranges from 10 to 750 ml/min with a discreteness of 1 ml/min. Pressure ranges — from 0.001 to 0.40 MPa with a discreteness of 0.0001 MPa. Deviation of the carrier gas flow rate from the average value of ± 1.5% in the flow range from 50 to 100 ml/min and ± 0.5 ml/min in the flow range from 3 to 50 ml/min. The relative deviation of the average steady-state gas flow rate from the set value in the range: from 3 to 100 ml/min. ± 2.5%, but not less than 0.5 ml/min.; from 100 to 200 ml/min. ± 5%; from 200 to 800 ml/min. ± 10%. Electric power supply from a single—phase AC network with voltage from 187 to 242 V, frequency (50 ± 1) Hz, operating mode - continuous. Power consumption, no more than — 30 VA. Overall dimensions of the FGP (width × depth × height), no more than 160 × 370× 210 mm. Weight, not more than — 8 kg.

Laboratory installation for modeling the process of thermal contact cracking (TCC) of heavy oil residues (TNO) (heavy oil fuel oil, tar and semi-tar, asphalt of the process of de-asphalting of high-viscosity oils, cracking residue or pitch, heavy gas oil, natural bitumen, etc.) with a movable solid coolant. technical specifications Operating pressure range, MPa 0÷4 Reactor operating temperature range, 0C 50÷800 Reactor inner diameter, mm, 31 Reactor length, mm, 875 Number of thermostatically controlled independent zones 4 Length of each independent isothermal zone of the furnace, mm 200 The length of the full isothermal zone of the furnace, mm 800 Thermocouple Pocket Availability The type of furnace is Casement The power consumed by each independent thermostatically controlled zone of the furnace, W 720 Power consumed by all four zones of the furnace, W 2880 The discreteness of the temperature setting, 0C 1 The flow range of the liquid pump, ml/min 0.1-10 The maximum pressure of the high-pressure liquid pump, not less than 20 MPa Flow range N2, l/min 0÷20 Pressure in the low pressure lines N2 and air, MPa ≤0.6 Operating temperature range of the evaporator-mixer of raw materials, sup>0C 50÷500 Actuation pressure of mechanical safety valves, MPa 3 Maximum pressure in the raw material container, 0.1 MPa Supply voltage 230-240V 60Hz The power consumption of the installation is not more than 3.5 kW The discreteness of the temperatures and flow rates displayed on the displays is 0.1 Installation weight without cabinet, kg 100 Overall dimensions of the installation, mm 1900x865x550 Overall dimensions of the cabinet, mm 2000x880x800 The technical characteristics of the purchased units used in the installation are given in the technical documentation for these units supplied with the installation The length of the supply pipelines, m 10 The coolant of the refrigerator "tosol"

The KOV-4 type air compressor is designed to supply flame detectors of gas chromatographs with air. Technical specifications: Capacity, at least, l/min 3 Outlet air pressure, 0.25+5 MPa% Pressure stability at constant flow rate, not more than 0.0007 MPa Engine power consumption, max, VA 100 Receiver volume, l 9 Noise level, no more, 60 dBa Weight, not more than, kg 19 Overall dimensions (width×depth×height), not more than, mm 235×755×440 Single-phase mains voltage 220 V, 50 Hz

When analyzing gases dissolved in transformer oil using the ARP method (equilibrium vapor analysis), it is necessary to first fill a syringe with transformer oil with a carrier gas, and then, after achieving an equilibrium distribution of gases dissolved in oil between the liquid and gas phases, introduce the gas phase into the chromatograph (blow out the doses of the chromatograph dispenser tap). Moreover, the operations of filling the syringe and entering the sample are performed without air access. When filling the syringe, it is possible to fix the syringe stem at a certain volume. technical specifications The volume of syringes is 20 or 50 ml. The pressure at the outlet of the syringe filling line with argon is 0.5 atm. The range of ratios of volumes of the gas phase and oil (Vg/Vm) is from 0 to 1.5.